By M.J. Forrest
This evaluation outlines every one strategy utilized in plastics research after which illustrates which tools are utilized to acquire a specific end result or piece of compositional details. for instance, polymer and filler identity, molecular weight selection, antidegradant quantification and floor research learn equipment are all incorporated. round four hundred abstracts from the Rapra Polymer Library database accompany this evaluate, to facilitate additional interpreting.
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Extra resources for Analysis of Plastics, Vol. 13 (2002)(en)(160s)
Sidwell, Plastics and Rubber International, 1983, 8, 6, 15. L. Koenig, Spectroscopy of Polymers, Elsevier, 1999. R Crompton, Manual of Plastics Analysis, Plenum, 1998. R. Crompton, Practical Polymer Analysis, Plenum Press, 1993. H. Fawcett, Wiley, 1996. 7 J. A. M. Squirrell, Identification and Analysis of Plastics, 2nd Edition, Butterworth, 1972. J. Wyatt, Analytica Chimica Acta, 1992, 272, 1. O. Hummel, Atlas of Polymer and Plastics Analysis, Volume 2, Carl Hanser Verlag, 1984. D. Page, Journal of Chromatographic Science, 1979, 17, 188.
The LC-MS technique therefore compliments GC-MS and, with it, enables the complete molecular weight/volatility/polarity range to be covered. (2) Irganox 1098 (3) Irganox 1076 (4) Irganox 1330 (5) Butylated hydroxytoluene (6) Irgafos 168 (7) Triclosan TLC is comparatively easy and cheap to use and it is both quick and accurate for the identification of Figure 13 HPLC chromatogram of a complex mixture of antidegradants 23 Analysis of Plastics antioxidants in plastic extracts. Irrespective of the complexity of the extract composition and the amount used, this method can be used to give a sharp separation for identification purposes.
In the thermal analysis field, a number of developments have occurred in recent years, with modulated temperature forms of TGA, DSC and TMA being brought out by manufacturers. Modulating the temperature enables these techniques to deliver better, more informative data on samples. Another development within the thermal analysis group is the micro-thermal analysis (micro-TA) instrument. This technique combines the topographical mapping capabilities of a scanning probe microscope with the ability to perform localised thermal analysis (DTA and TMA) on a micron scale.
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